関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Allylamine | HCID 7853 | — |
| 反応物 | [7-(Methylsulfonyl)-2,3-dihydro-1,4-benzodioxin-2-yl]methyl 4-methylbenzenesulfonate | HCID 86652933 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | N-{[7-(Methylsulfonyl)-2,3-dihydro-1,4-benzodioxin-2-YL]methyl}prop-2-EN-1-amine | HCID 44469735 | — |
反応手順
A mixture of [7-(methylsulfonyl)-2,3-dihydro-1,4-benzodioxin-2-yl]methyl 4-methylbenzenesulfonate (0.018 g, 0.046 mmol), prop-2-en-1-amine (0.5 ml) and ACN (3 ml) was heated under microwave radiation at 120° C. for 20 min. MS m/z (rel. intensity, 70 eV) 283 (M+, 4), 79 (4), 71 (6), 70 (bp), 68 (4).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08524766B2 |
|---|
| 出典データセット | uspto-grants-2013_09 |
|---|
| ORD ID | ord-c16cad3b0ed0401b80120fb8c41e1275 |
|---|
| 出典メモ | uspto-grants-2013_09 |
|---|
