関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 1,4-Dichlorobenzene | HCID 4685 | — |
| 反応物 | 3H-Indole, 2,3,3-trimethyl- | HCID 15427 | — |
| 反応物 | 1-Bromo-3,6-dioxaheptane | HCID 123532 | — |
| 生成物 | 1-(2-(2-Methoxyethoxy)ethyl)-2,3,3-trimethyl-3h-indolium bromide | HCID 68813660 | — |
反応手順
To 2,3,3-trimethylindolenine (1.59 g) was added 1-bromo-2-(2-methoxyethoxy)ethane (2.75 g) and dichlorobenzene (5 ml). The mixture was heated to 70° C. overnight. The volatiles were stripped and the material purified by HPLC.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08378120B2 |
|---|
| 出典データセット | uspto-grants-2013_02 |
|---|
| ORD ID | ord-d7d322c6a96a4247a8c483bed3a38135 |
|---|
| 出典メモ | uspto-grants-2013_02 |
|---|
