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p-Toluenesulfonic acid → 1-Acetoxy-3-(8,11,14-pentadecatrienyl) benzene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | p-Toluenesulfonic acid | HCID 6101 | — |
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 反応物 | Cardanol | HCID 11266523 | — |
| 生成物 | 1-Acetoxy-3-(8,11,14-pentadecatrienyl) benzene | HCID 69049096 | — |
反応手順
A mixture of acetic anhydride (0.1 mol, 15 ml) and p-toluenesulphonic acid (PTSA, 3.15 mol %, 0.6 g) were taken in a two necked RB flask and double distilled cardanol (0.1 mol, 30 g) was added dropwise with stirring over a period of 30 minutes at ambient conditions. The reaction was continued for 8-12 h. The product (AC) was washed free of acetic acid and catalyst with water and dried.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08378135B2 |
| 出典データセット | uspto-grants-2013_02 |
| ORD ID | ord-eef7ad41575b4ffdbb03c5667438d682 |
| 出典メモ | uspto-grants-2013_02 |