戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 389345作成日:2026年10月26日

p-Toluenesulfonic acid → 1-Acetoxy-3-(8,11,14-pentadecatrienyl) benzene

https://huagongshe.com/reaction/389345

反応式

関与物質

役割名称HCID仕込み量
反応物p-Toluenesulfonic acidHCID 6101—
反応物Acetic AnhydrideHCID 7918—
反応物CardanolHCID 11266523—
生成物1-Acetoxy-3-(8,11,14-pentadecatrienyl) benzeneHCID 69049096—

反応手順

A mixture of acetic anhydride (0.1 mol, 15 ml) and p-toluenesulphonic acid (PTSA, 3.15 mol %, 0.6 g) were taken in a two necked RB flask and double distilled cardanol (0.1 mol, 30 g) was added dropwise with stirring over a period of 30 minutes at ambient conditions. The reaction was continued for 8-12 h. The product (AC) was washed free of acetic acid and catalyst with water and dried.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08378135B2
出典データセットuspto-grants-2013_02
ORD IDord-eef7ad41575b4ffdbb03c5667438d682
出典メモuspto-grants-2013_02