化工社化工社 化学情報印刷レポート · 研究参考用
2-Acrylamido-2-methyl-1-propanesulfonic acid → Ammonium acryloyldimethyltaurate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Acrylamido-2-methyl-1-propanesulfonic acid | HCID 65360 | — |
| 反応物 | Ethanamine, 2-(2-methoxyethoxy)-N,N-bis[2-(2-methoxyethoxy)ethyl]- | HCID 112414 | — |
| 生成物 | Ammonium acryloyldimethyltaurate | HCID 6850854 | 99% |
反応手順
A nitrogen purged 50 ml schlenk flask was charged with freshly distilled tris[2-(2-methoxyethoxy)-ethyl]amine (1.69 g, 5.24 mmol) and 2-acrylamido-2-methyl-1-propanesulfonic acid (AMPS) (1.09 g, 5.24 mmol) and stirred at ambient temperature for 8 hr or until completely dissolved. Total dissolution completes formation of the AMPS-ammonium salt monomer as a transparent light amber oil in a 99% yield which was used immediately without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | USRE044032E1 |
| 出典データセット | uspto-grants-2013_02 |
| ORD ID | ord-f8b9578b9867420d8964739d7569bf17 |
| 出典メモ | uspto-grants-2013_02 |