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3-(2-Chlorophenyl)propanoic acid → 2-(7-Chloro-1'-(3-(2-chlorophenyl)propanoyl)-2,3-dihydrospiro[indene-1,4'-piperidine]-3-yl)acetic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-(2-Chlorophenyl)propanoic acid | HCID 95676 | — |
| 反応物 | Ethyl 2-(7-chloro-2,3-dihydrospiro[indene-1,4'-piperidine]-3-yl)acetate | HCID 67224803 | — |
| 生成物 | 2-(7-Chloro-1'-(3-(2-chlorophenyl)propanoyl)-2,3-dihydrospiro[indene-1,4'-piperidine]-3-yl)acetic acid | HCID 58295673 | — |
反応手順
The title compound was prepared following a procedure analogous to that described in Example 1 using 3-(2-chlorophenyl)propanoic acid and ethyl 2-(7-chloro-2,3-dihydrospiro[indene-1,4′-piperidine]-3-yl)acetate followed by a procedure analogous to that in Example 2. LC-MS Method 1 tR=1.87, min, m/z=446
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08383629B2 |
| 出典データセット | uspto-grants-2013_02 |
| ORD ID | ord-303b22150aca4edc9c24f486f8152fec |
| 出典メモ | uspto-grants-2013_02 |