Benzoyl chloride, 3-bromo- → HCID 25054619、化合物
反応式
N1N[N:3]=[N:4][C:5]=1[C:6]1[CH:7]=[N:8][CH:9]=[CH:10][CH:11]=1.[Br:12][C:13]1[CH:14]=[C:15]([CH:19]=[CH:20][CH:21]=1)[C:16](Cl)=[O:17]>CC1C=CC=CC=1C>[Br:12][C:13]1[CH:14]=[C:15]([C:16]2[O:17][C:5]([C:6]3[CH:7]=[N:8][CH:9]=[CH:10][CH:11]=3)=[N:4][N:3]=2)[CH:19]=[CH:20][CH:21]=1参加物
4
実験手順
16.8 g (114 mmol) of 3-(2H-tetrazol-5-yl)pyridine) according to Synthesis Example 7 and 25 g (114 mmol) of 3-bromobenzoylchloride were dissolved in 180 mL of o-xylene. The solution was reacted at 150° C. for 8 hours. The acquired reactant was purified under reduced pressure and washed with methanol, obtaining 30 g (Y=87%) of a white solid.
後処理
- customThe solution was reacted at 150° C. for 8 hours
- customThe acquired reactant was purified under reduced pressure
- washwashed with methanol
- customobtaining 30 g (Y=87%) of a white solid
出典と根拠
- ORDレコード
- ord-69451d115958415b9c722df003378e15
- 出典データセット
- uspto-grants-2013_02
- 特許番号
- US08383932B2
反応ノート
読み込み中…