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Acetone → Stearyl glycidyl ether octyl glycidyl ether
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetone | HCID 180 | — |
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Toluene | HCID 1140 | — |
| 反応物 | Glycidyl n-octyl ether | HCID 92955 | — |
| 生成物 | Stearyl glycidyl ether octyl glycidyl ether | HCID 86586154 | 75% |
反応手順
50 mL of Catalyst B, 40.0 g of stearyl glycidyl ether (SGE) and 22.8 g of octyl glycidyl ether (OGE) were added to 210 ml of toluene, and a vessel was closed. The polymerization was carried out at 130° C. for 24 hours with stirring. The reaction solution was added to a large amount of acetone containing a small amount of a dilute solution of hydrogen chloride. A precipitated solid was dried under reduced pressure at 80° C. for 24 hours to obtain a poly(stearyl glycidyl ether/octyl glycidyl ether) copolymer. Pale yellow solid. Yield 75%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06800723B2 |
| 出典データセット | uspto-grants-2004_10 |
| ORD ID | ord-9909a9a5f8c54061893a864b5514024b |
| 出典メモ | uspto-grants-2004_10 |