関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Dimethyl Sulfide | HCID 1068 | — |
| 反応物 | Dimethyl Sulfate | HCID 6497 | — |
| 反応物 | Sulfonium, trimethyl-, sulfate (1:1) | HCID 10942955 | — |
| 生成物 | Trimethylsulfonium methyl sulfate | HCID 2760871 | — |
反応手順
Synthesis of trimethysulfonium hydrogen sulfate: To dimethyl sulfate (10.0 mL, 1.05×10−1 mol) at 0° C. was added dimethyl sulfide (10.4 mL, 1.42×10−1 mol). After rapidly stirring at 0° C. for 30 minutes, the reaction was slowly warmed to room temperature yielding a crystalline solid, trimethylsulfonium methyl sulfate. After 3 hours, distilled water (20 mL) was added to form a clear solution of trimethylsulfonium sulfate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06800766B2 |
|---|
| 出典データセット | uspto-grants-2004_10 |
|---|
| ORD ID | ord-a8941cee5f4f42d68566fd502884c095 |
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| 出典メモ | uspto-grants-2004_10 |
|---|
