Phenol → 2,4-Di-(4-chloro-alpha-cumyl)phenol

HRID 392554

反応式

HRID 392554 の反応式
[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Cl:8][C:9]1[CH:17]=[CH:16][C:12]([C:13]([CH3:15])=[CH2:14])=[CH:11][CH:10]=1>>[Cl:8][C:9]1[CH:17]=[CH:16][C:12]([C:13]([C:2]2[CH:3]=[C:4]([C:13]([C:12]3[CH:16]=[CH:17][C:9]([Cl:8])=[CH:10][CH:11]=3)([CH3:15])[CH3:14])[CH:5]=[CH:6][C:1]=2[OH:7])([CH3:15])[CH3:14])=[CH:11][CH:10]=1

参加物

3

反応物 2

HCID 996PhenolHCID 743814-Chloro-alpha-methylstyrene

生成物 1

HCID 226643982,4-Di-(4-chloro-alpha-cumyl)phenol収率 66.2%

実験手順

The title compound is prepared according to the procedure of Example 3 by reacting 19 g of phenol with 80 g of 4-chloro-α-methylstyrene to give 53.4 g of the title compound as a white solid. The structure is confirmed by 1Hnmr and mass spectroscopy.

後処理

  1. customThe title compound is prepared

出典と根拠

ORDレコード
ord-c0eaf3df57e54f9382b58b89d4ccd2ca
出典データセット
uspto-grants-2004_10
特許番号
US06800676B2

関連ノート

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