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Thionyl Chloride → 2-Chlorotrityl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | (2-Chlorophenyl)diphenylmethanol | HCID 298659 | — |
| 生成物 | 2-Chlorotrityl chloride | HCID 94524 | 82% |
反応手順
Following the procedure outlined in Example 4, 5.00 g (17.1 mmol) of (2-chlorophenyl) diphenyl methanol, designated as T-3 on Appendix A, was treated with 2.5 ml thionyl chloride (34 mmol) according to general method B to give 4.39 g (82%) of (2-Chlorophenyl) diphenyl chloromethane, mp: 131° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06803375B1 |
| 出典データセット | uspto-grants-2004_10 |
| ORD ID | ord-4d903e8bd7e34041a3d7ddc86464de98 |
| 出典メモ | uspto-grants-2004_10 |