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N,N,3-trimethyl-4-nitrobenzamide → 4-amino-N,N,3-trimethylbenzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N,N,3-trimethyl-4-nitrobenzamide | HCID 786992 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 4-amino-N,N,3-trimethylbenzamide | HCID 16781770 | — |
反応手順
N,N,3-trimethyl-4-nitrobenzamide (0.6 g, 2.88 mmol) in methanol was hydrogenated using the H-cube apparatus (1.2 mL/min, RT, atmospheric pressure). After 45 minutes the reaction was complete. Removal of the solvent in vacuo gave 4-amino-N,N,3-trimethylbenzamide as a colourless solid (quantitative); MS (ES+) 179.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08524902B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-3fa264f9a8bd4375af3bdd364a61e69a |
| 出典メモ | uspto-grants-2013_09 |