化工社化工社 化学情報印刷レポート · 研究参考用
Methyl cyclohexanecarboxylate → Methyl 1-(iodomethyl)cyclohexanecarboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl cyclohexanecarboxylate | HCID 20748 | — |
| 反応物 | 4-Iodomethyl-tetrahydro-pyran-4-carboxylic acid methyl ester | HCID 22719788 | — |
| 生成物 | Methyl 1-(iodomethyl)cyclohexanecarboxylate | HCID 58947958 | 100% |
反応手順
Prepared according to the method for the preparation of 4-iodomethyltetrahydropyran-4-carboxylic acid methyl ester, from cyclohexane-carboxylic acid methyl ester (10 ml), to give the title compound as a brown gum (20 g, 100%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06809100B2 |
| 出典データセット | uspto-grants-2004_10 |
| ORD ID | ord-ddacfc71a8504682a05627c6e4b3745c |
| 出典メモ | uspto-grants-2004_10 |