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Methyl 4-[(acetylsulfanyl)methyl]oxane-4-carboxylate → 1-Acetylsulfanylmethylcyclohexanecarboxylic acid methyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl 4-[(acetylsulfanyl)methyl]oxane-4-carboxylate | HCID 23448262 | — |
| 反応物 | Methyl 1-(iodomethyl)cyclohexanecarboxylate | HCID 58947958 | — |
| 生成物 | 1-Acetylsulfanylmethylcyclohexanecarboxylic acid methyl ester | HCID 58947950 | 92% |
反応手順
Prepared according to the method for the preparation of 4-acetylsulfanylmethyltetrahydropyran-4-carboxylic acid methyl ester, from 1-iodomethylcyclohexanecarboxylic acid methyl ester (20 g), to yield the title compound as a brown gum (15 g, 92%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06809100B2 |
| 出典データセット | uspto-grants-2004_10 |
| ORD ID | ord-f1fc7002919e45578ab70aacfdbdf934 |
| 出典メモ | uspto-grants-2004_10 |