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Hydrochloride methanol → Ethyl 3-{(2-aminoacetyl)amino}propionate monohydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloride methanol | HCID 21893726 | — |
| 反応物 | Ethyl 3-(2-{(tert-butoxycarbonyl)amino}acetylamino)propionate | HCID 21893946 | — |
| 生成物 | Ethyl 3-{(2-aminoacetyl)amino}propionate monohydrochloride | HCID 22647362 | — |
反応手順
2.0 Grams of ethyl 3-(2-{(tert-butoxycarbonyl)amino}acetylamino)propionate were dissolved in 30 ml of 10% hydrochloric acid-methanol and stirred for 15 hours at room temperature. Upon distilling the reaction liquid off under reduced pressure, 1.52 g of the title compound was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06809108B1 |
| 出典データセット | uspto-grants-2004_10 |
| ORD ID | ord-f6acccc2d5c9469da199616aa179c473 |
| 出典メモ | uspto-grants-2004_10 |