化工社化工社 化学情報印刷レポート · 研究参考用
Aluminium lithium hydride → 3-(2-Phenyl-thiazol-4-yl)-propan-1-ol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aluminium lithium hydride | HCID 21226445 | — |
| 反応物 | 3-(2-Phenyl-thiazol-4-yl)-propionic acid ethyl ester | HCID 68616668 | — |
| 生成物 | 3-(2-Phenyl-thiazol-4-yl)-propan-1-ol | HCID 22647495 | 76% |
反応手順
In analogy of the procedure described in example 12 b], 0.44 g (1.68 mmol) of 3-(2-phenyl-thiazol-4-yl)-propionic acid ethyl ester was reacted with lithium aluminium hydride, yielding 0.28 g of 3-(2-phenyl-thiazol-4-yl)-propan-1-ol as colorless liquid (75.8% of theory).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06809110B2 |
| 出典データセット | uspto-grants-2004_10 |
| ORD ID | ord-07277705a0cd4d4985dca79089eb6c04 |
| 出典メモ | uspto-grants-2004_10 |