化工社化工社 化学情報印刷レポート · 研究参考用
Acetic Acid → Phthalic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | Phthalic Anhydride | HCID 6811 | — |
| 反応物 | O-Xylene | HCID 7237 | — |
| 生成物 | Phthalic Acid | HCID 1017 | — |
| 生成物 | Phthalic Anhydride | HCID 6811 | — |
反応手順
As an example, reference is made to the production of phthalic anhydride with acetic acid as solvent. During oxidation of o-xylene as feedstock, phthalic acid and phthalic anhydride are obtained as products in the liquid-phase reactor. Therefore, not only the binary crystallization curves of phthalic acid in acetic acid or phthalic anhydride in acetic acid are used, but also those of the ternary system phthalic acid/phthalic anhydride/in acetic acid. By using the process of the invention, phthalic acid and phthalic anhydride are obtained as pure solid products. The acetic acid obtained as byproduct is recirculated into the reactor as solvent.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08524922B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-98b5a59ed8fd4b229550e2884de4185c |
| 出典メモ | uspto-grants-2013_09 |