2,3-Dimethoxyaniline → 1-(Tert-butoxycarbonyl)-4-(2,3-dimethoxyphenylamino)piperidine

HRID 395528

反応式

HRID 395528 の反応式
[C:1]([O:5][C:6]([N:8]1[CH2:13][CH2:12][C:11](=O)[CH2:10][CH2:9]1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[CH3:15][O:16][C:17]1[C:23]([O:24][CH3:25])=[CH:22][CH:21]=[CH:20][C:18]=1[NH2:19]>>[C:1]([O:5][C:6]([N:8]1[CH2:13][CH2:12][CH:11]([NH:19][C:18]2[CH:20]=[CH:21][CH:22]=[C:23]([O:24][CH3:25])[C:17]=2[O:16][CH3:15])[CH2:10][CH2:9]1)=[O:7])([CH3:4])([CH3:3])[CH3:2]

参加物

3

反応物 2

HCID 2396032,3-DimethoxyanilineHCID 735900tert-Butyl 4-oxopiperidine-1-carboxylate

生成物 1

HCID 225578701-(Tert-butoxycarbonyl)-4-(2,3-dimethoxyphenylamino)piperidine

実験手順

1-(tert-Butoxycarbonyl)-4-piperidone (4.78 g) and 2,3-dimethoxyaniline (3.68 g) were condensed in the same manner as described in Preparation Example 37 to give the title compound.

後処理

  1. customcondensed in the same manner
  2. customas described in Preparation Example 37

出典と根拠

ORDレコード
ord-2d60edcda598439db59e5a80ea3ebd75
出典データセット
uspto-grants-2003_08
特許番号
US06605620B1

関連ノート

読み込み中…