3-Benzyloxyaniline → 2-[(4-Tert-butylbenzoyl)amino]-n-(3-benzyloxyphenyl)-5-nitrobenzamide
反応式
[CH2:1]([O:8][C:9]1[CH:10]=[C:11]([CH:13]=[CH:14][CH:15]=1)[NH2:12])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:16]([C:20]1[CH:25]=[CH:24][C:23]([C:26]2[O:31][C:30](=[O:32])[C:29]3[CH:33]=[C:34]([N+:37]([O-:39])=[O:38])[CH:35]=[CH:36][C:28]=3[N:27]=2)=[CH:22][CH:21]=1)([CH3:19])([CH3:18])[CH3:17]>>[C:16]([C:20]1[CH:25]=[CH:24][C:23]([C:26]([NH:27][C:28]2[CH:36]=[CH:35][C:34]([N+:37]([O-:39])=[O:38])=[CH:33][C:29]=2[C:30]([NH:12][C:11]2[CH:13]=[CH:14][CH:15]=[C:9]([O:8][CH2:1][C:2]3[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=3)[CH:10]=2)=[O:32])=[O:31])=[CH:22][CH:21]=1)([CH3:19])([CH3:17])[CH3:18]参加物
3
実験手順
Using the procedure described in Example 91, Part B, 3-benzyloxyaniline (2.5 mmol) and 2-(4-tert-butylphenyl)-6-nitro-4H-3,1-benzoxazin-4-one (2.8 mmol) yielded 550 mg (42%) of the title compound.
出典と根拠
- ORDレコード
- ord-4ae91a49d59f4d7ca3194e0b05198f68
- 出典データセット
- uspto-grants-2003_08