関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Benzene | HCID 241 | — |
| 反応物 | Propylene | HCID 8252 | — |
| 生成物 | Cumene | HCID 7406 | — |
反応手順
All experiments were conducted in a fixed-bed, ⅜″ or ¾″ OD tubular reactor in a downflow configuration. The reactor furnace was controlled in isothermal mode. The catalyst was dried off-line at 260° C. in air for two hours before loading. Experiments were conducted with catalyst as whole extrudates loaded into the ⅜″ reactor. The catalyst bed was axially centered in the middle furnace zone. The catalyst was used extrudate form or crushed and sized to 50-60 mesh depending on the type of experiment. All catalysts were packed with inert sand to fill the interstitial void spaces. Reaction conditions were 125° C., benzene:propylene molar ratio of 2.8, and 31887 kPa-a (300 psig). Weight Hourly Space Velocity was adjusted during the experiments and ranged from 1 h−1 WHSV (propylene basis) to 320 h−1 WHSV (propylene basis).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US08524967B2 |
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| 出典データセット | uspto-grants-2013_09 |
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| ORD ID | ord-f5e3a49c84ba41b6901478019fa7c644 |
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| 出典メモ | uspto-grants-2013_09 |
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