Carbon tetrabromide → (Bromomethyl)cycloheptane

反応式

[CH:1]1([CH2:8]O)[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C(Br)(Br)(Br)[Br:11]>>[Br:11][CH2:8][CH:1]1[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

参加物

反応物 2

HCID 11205Carbon tetrabromide

HCID 78193Cycloheptanemethanol

生成物 1

HCID 23000753(Bromomethyl)cycloheptane

実験手順

The subtitle compound was prepared by the method of Preparation 9 from cycloheptylmethanol and carbon tetrabromide. The crude product was purified by fractional distillation, b.pt. 115° C.-120° C. @ 30mmHg to afford 1-(bromomethyl)cycloheptane as an oil.

後処理

distillationThe crude product was purified by fractional distillation, b.pt. 115° C.-120° C.

出典と根拠

ORDレコード: ord-082a997b385e4a4ea28cd2683bd2593d
出典データセット: uspto-grants-2003_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06610707B1

反応ノート

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