Formic Acid → Methyl 3-formamidocinnamate
反応式
[NH2:1][C:2]1[CH:3]=[C:4]([CH:11]=[CH:12][CH:13]=1)[CH:5]=[CH:6][C:7]([O:9][CH3:10])=[O:8].[CH:14](O)=[O:15]>O>[CH:14]([NH:1][C:2]1[CH:3]=[C:4]([CH:11]=[CH:12][CH:13]=1)[CH:5]=[CH:6][C:7]([O:9][CH3:10])=[O:8])=[O:15]参加物
4
実験手順
193 g of methyl 3-aminocinnamate and 900 ml of formic acid were mixed and heated under reflux for 2 hours. The reaction solution was poured into water and the crystals (methyl 3-formamidocinnamate) obtained were collected by filtration. Yield: 127 g.
後処理
- temperatureheated
- temperatureunder reflux for 2 hours
出典と根拠
- ORDレコード
- ord-544208453dae4717be0d51f4b646578f
- 出典データセット
- uspto-grants-1998_10
- 特許番号
- US05827638
反応ノート
読み込み中…