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Acetyl chloride → Methyl 3-(3-bromophenyl)prop-2-enoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetyl chloride | HCID 6367 | — |
| 反応物 | 3-(3-Bromophenyl)acrylic acid | HCID 36251 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Methyl 3-(3-bromophenyl)prop-2-enoate | HCID 610698 | — |
反応手順
To a solution of 50.0 g (220 mmol, Aldrich) of 3-bromocinnamic acid in 1 L sieve-dried methanol (Burdick & Jackson), stirred at 0° C., was added dropwise a solution of acidic methanol (prepared by the addition of 2.5 mL acetyl chloride to 250 mL methanol). The reaction
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05827868 |
| 出典データセット | uspto-grants-1998_10 |
| ORD ID | ord-f8d184a5c3014a92bc4fb77c554723dc |
| 出典メモ | uspto-grants-1998_10 |