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4-Hydroxy-4'-nitrobiphenyl → N,N-bis-(isopropyl)-2[[4'-nitro-(1,1'-biphenyl)-4-yl]oxy]-acetamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Hydroxy-4'-nitrobiphenyl | HCID 138078 | — |
| 反応物 | 2-Bromo-N,N-diisopropylacetamide | HCID 10900191 | — |
| 生成物 | N,N-bis-(isopropyl)-2[[4'-nitro-(1,1'-biphenyl)-4-yl]oxy]-acetamide | HCID 21841479 | 84.5% |
反応手順
The product was prepared as in Example 2, Stage A starting with 900 mg of 4'-hydroxy-(4-nitro biphenyl) (Aldrich) and 958 mg of N,N-bis-(isopropyl)-2-bromo-acetamide (Preparation 8) to obtain 1.26 g of the expected product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05827887 |
| 出典データセット | uspto-grants-1998_10 |
| ORD ID | ord-4b1bbf3a66324fc88b583320d996d174 |
| 出典メモ | uspto-grants-1998_10 |