化工社化工社 化学情報印刷レポート · 研究参考用
Water → HCID 178497263、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Hydrazine, acetate (1:1) | HCID 165591 | — |
| 反応物 | Methyl 2,4-dioxo-4-phenylbutanoate | HCID 308117 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | HCID 178497263 | HCID 178497263 | 66.3% |
反応手順
983 mg hydrazine acetate was added to 2 g 2,4-Dioxo-4-phenyl-butyric acid methyl ester in 10 mL concentrated acetic acid. The mixture was stirred over night at RT. Then water was added. The precipitate was filtered, stirred with diisopropylether and again filtered to give 1.3 g desired product. Rt: 1.39 min (method O), (M+H)+: 203
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08741892B2 |
| 出典データセット | uspto-grants-2014_06 |
| ORD ID | ord-8ffbecc03032464c90cc429146c8e351 |
| 出典メモ | uspto-grants-2014_06 |