化工社化工社 化学情報印刷レポート · 研究参考用
Ethylacetate heptane → 6-chloro-N-methyl-4-phenylpyridazin-3-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethylacetate heptane | HCID 21899848 | — |
| 反応物 | 6-Chloro-4-phenylpyridazin-3-amine | HCID 76848713 | — |
| 生成物 | 6-chloro-N-methyl-4-phenylpyridazin-3-amine | HCID 86698478 | — |
反応手順
The title compound was prepared in analogy to example 1, intermediate a, from 6-chloro-4-phenyl-pyridazin-3-ylamine and using a gradient of n-heptane:ethyl acetate (100:0 to 40:60) for the chromatographic purification. Light yellow solid (52%). MS (ESI+): m/z=220.064 ([M+H]+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08748434B2 |
| 出典データセット | uspto-grants-2014_06 |
| ORD ID | ord-7e66c99393e84a34bdda062980d3e56e |
| 出典メモ | uspto-grants-2014_06 |