Oxolan-3-yl methanesulfonate → 4-bromo-1-(oxolan-3-yl)-1H-pyrazole

反応式

[Br:1][C:2]1[CH:3]=[N:4][N:5]([CH:7]2[CH2:10][CH2:9][CH2:8]2)[CH:6]=1.CS(OC1CCOC1)(=O)=[O:13]>>[Br:1][C:2]1[CH:3]=[N:4][N:5]([CH:7]2[CH2:10][CH2:9][O:13][CH2:8]2)[CH:6]=1

参加物

反応物 2

HCID 15278452Oxolan-3-yl methanesulfonate

HCID 665214554-Bromo-1-cyclobutylpyrazole

生成物 1

HCID 592316834-bromo-1-(oxolan-3-yl)-1H-pyrazole

実験手順

The title compound was prepared in the same manner as 4-bromo-1-(cyclobutyl)-1H-pyrazole, but using tetrahydrofuran-3-yl methanesulfonate (prepared according to procedures known in the art).

後処理

customprepared

出典と根拠

ORDレコード: ord-015c95e94c6048b081c3b3e69fedc934
出典データセット: uspto-grants-2013_09
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08524900B2

反応ノート

読み込み中…