化工社化工社 化学情報印刷レポート · 研究参考用
Hydroxide → Diphenyldiethylphosphonium hydroxide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydroxide | HCID 961 | — |
| 反応物 | Phosphonium, diethyldiphenyl-, iodide | HCID 357429 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Diphenyldiethylphosphonium hydroxide | HCID 18407746 | 96% |
反応手順
This 98.45 g of diphenyldiethylphosphonium iodide was then dissolved in water, and converted to the corresponding hydroxide with 270 g of an anionic exchange resin in batch overnight, yielding 271.75 g of a 0.94 M solution of diphenyldiethylphosphonium hydroxide (96% of exchange yield) The diphenyldiethylphosphonium hydroxide was used as SDA source.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08529868B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-2249a546e80243079730b7f18d3febb6 |
| 出典メモ | uspto-grants-2013_09 |