4-Bromo-3-chlorobenzaldehyde → (4-Bromo-3-chloro-benzyl)-(2,2-dimethoxy-ethyl)-amine

反応式

[Br:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=O)=[CH:4][C:3]=1[Cl:10].BrC1C=CC(C[NH:17][CH2:18][CH:19]([O:22][CH3:23])[O:20][CH3:21])=CC=1>>[Br:1][C:2]1[CH:9]=[CH:8][C:5]([CH2:6][NH:17][CH2:18][CH:19]([O:22][CH3:23])[O:20][CH3:21])=[CH:4][C:3]=1[Cl:10]

参加物

反応物 2

HCID 140498064-Bromo-3-chlorobenzaldehyde

HCID 59226241N-(4-Bromobenzyl)-2,2-dimethoxyethanamine

生成物 1

HCID 59226250(4-Bromo-3-chloro-benzyl)-(2,2-dimethoxy-ethyl)-amine

実験手順

Starting from 4-Bromo-3-chloro-benzaldehyde, the title compound was prepared by the method described for (4-Bromo-benzyl)-(2,2-dimethoxy-ethyl)-amine (1). Rt=0.94 min (Method C). Detected mass: 308.3/310.3 (M+H+).

出典と根拠

ORDレコード: ord-f376babee88648508d34c85d466a6ed3
出典データセット: uspto-grants-2014_06
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08748614B2

反応ノート

読み込み中…