Hydrochloric Acid → HCID 68592442、化合物
反応式
BrC1C=C2C(C=CN=C2)=CC=1[Cl:12].[Br:13][C:14]1[CH:23]=[C:22]2[C:17]([CH:18]=[CH:19][N:20]=[CH:21]2)=[CH:16][C:15]=1[S:24][CH2:25][CH:26]1[CH2:31][CH2:30][CH2:29][NH:28][CH2:27]1.C(OC(N1CCCC(CBr)C1)=O)(C)(C)C.Cl>>[ClH:12].[Br:13][C:14]1[CH:23]=[C:22]2[C:17]([CH:18]=[CH:19][N:20]=[CH:21]2)=[CH:16][C:15]=1[S:24][CH2:25][CH:26]1[CH2:31][CH2:30][CH2:29][NH:28][CH2:27]1参加物
4
実験手順
Starting from 7-Bromo-6-chloroisoquinoline (265) and 3-Bromomethyl-piperidine-1-carboxylic acid tert-butyl ester 7-Bromo-6-(piperidin-3-ylmethylsulfanyl)-isoquinoline could be obtained according to the procedures described for 272, 267, 268 as the hydrochloride. Rt=0.82 min (Method B). Detected mass: 337.1 (M+H+).
後処理
- customcould be obtained