反応式
[Cl:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[N:8]=[C:7]([CH3:12])[CH:6]=[CH:5]2.[O:13]1CCOCC1>>[Cl:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[N:8]=[C:7]([CH:12]=[O:13])[CH:6]=[CH:5]2参加物
3
反応条件
- 温度
- 80 °C
実験手順
A suspension of 6-chloro-2-methyl-quinoline (355 mg) and SeO2 (233 mg) in 1,4-dioxane (3 mL) was heated at 80° C. for 16 h. The resulting black mixture was filtered through diatomaceous earth. Concentration of the filtrate gave the title compound as a yellow powder (324 mg).
後処理
- filtrationThe resulting black mixture was filtered through diatomaceous earth
出典と根拠
- ORDレコード
- ord-2952c511f0834aa6ab9efb4ef46915e5
- 出典データセット
- uspto-grants-2013_09
- 特許番号
- US08530476B2
関連ノート
読み込み中…