化工社化工社 化学情報印刷レポート · 研究参考用
Methylamine → n-Methyl-3-nitropyridin-4-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methylamine | HCID 6329 | — |
| 反応物 | 4-Methoxy-3-nitropyridine | HCID 355832 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | n-Methyl-3-nitropyridin-4-amine | HCID 556016 | — |
反応手順
2.36 g 4-methoxy-3-nitro-pyridine and 2.33 ml methylamine (40% in water) are refluxed in 25 ml of ethanol for 3 h. Then the reaction mixture is evaporated to dryness. 2.3 g product are obtained as a solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08754073B2 |
| 出典データセット | uspto-grants-2014_06 |
| ORD ID | ord-35e601a38c5e47dfb5ec3c8613cdef1f |
| 出典メモ | uspto-grants-2014_06 |