化工社化工社 化学情報印刷レポート · 研究参考用
1-Piperonylpiperazine → 4-Benzo[1,3]dioxol-5-ylmethyl-piperazine-1-carboxylic acid pyridin-3-ylamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Piperonylpiperazine | HCID 94426 | — |
| 反応物 | Phenyl pyridin-3-ylcarbamate | HCID 6935890 | — |
| 生成物 | 4-Benzo[1,3]dioxol-5-ylmethyl-piperazine-1-carboxylic acid pyridin-3-ylamide | HCID 24528648 | — |
反応手順
The title compound was prepared from 1-benzo[1,3]dioxol-5-ylmethyl-piperazine and pyridin-3-yl-carbamic acid phenyl ester in analogy with Example 142. 1H NMR (400 MHz, CDCl3): 8.44-8.43 (m, 1H), 8.19-8.17 (m, 1H), 7.98-7.95 (m, 1H), 7.18-7.16 (m, 1H), 6.83-6.80 (m, 2H), 6.70 (s, 1H), 5.89 (s, 2H), 3.55-3.52 (m, 4H), 3.47 (s, 2H), 2.51-2.48 (m, 4H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08530476B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-2b34314bed5d49e6bd552f22b8d3f2fa |
| 出典メモ | uspto-grants-2013_09 |