化工社化工社 化学情報印刷レポート · 研究参考用
4-Methoxyphenol → 4-Methoxycyclohexanol (cis,trans)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Methoxyphenol | HCID 9015 | — |
| 反応物 | HCID 178418361 | HCID 178418361 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 4-Methoxycyclohexanol (cis,trans) | HCID 140332 | — |
反応手順
4-Methoxyphenol (100 g) in ethanol (759 ml) was hydrogenated under 50 psi hydrogen using Nishimura catalyst (10.0 g) at rt for 4.5 h. The catalyst was filtered off; the solvent was removed in vacuo to yield the desired product as 95% pure yellowish liquid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08754079B2 |
| 出典データセット | uspto-grants-2014_06 |
| ORD ID | ord-66c84cbcff4b405b833f38f35bbb2adf |
| 出典メモ | uspto-grants-2014_06 |