4-Methoxyphenol → 4-Methoxycyclohexanol (cis,trans)

HRID 406050

反応式

HRID 406050 の反応式
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([OH:9])=[CH:5][CH:4]=1.[H][H]>C(O)C>[CH3:1][O:2][CH:3]1[CH2:8][CH2:7][CH:6]([OH:9])[CH2:5][CH2:4]1

参加物

4

反応物 2

HCID 90154-MethoxyphenolHCID 178418361HCID 178418361、化合物

生成物 1

HCID 1403324-Methoxycyclohexanol (cis,trans)

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

A mixture of 100 g 4-methoxyphenol and Nishimura's catalyst in 750 ml ethanol were hydrogenated (50 psi hydrogen) at room temperature for 4.5 hours. The mixture was filtered and the filtrate was concentrated.

後処理

  1. customat room temperature
  2. customfor 4.5 hours
  3. filtrationThe mixture was filtered
  4. concentrationthe filtrate was concentrated

出典と根拠

ORDレコード
ord-eb53658046a44dc08b8875ac0fe90b71
出典データセット
uspto-grants-2014_06
特許番号
US08754079B2

関連ノート

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