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3,4-Dichlorobenzaldehyde → 4-(3,4-Dichloro-benzyl)-piperazine-1-carboxylic acid phenylamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,4-Dichlorobenzaldehyde | HCID 22710 | — |
| 反応物 | N-phenylpiperazine-1-carboxamide | HCID 7015289 | — |
| 生成物 | 4-(3,4-Dichloro-benzyl)-piperazine-1-carboxylic acid phenylamide | HCID 57880847 | — |
反応手順
The title compound was prepared from piperazine-1-carboxylic acid phenylamide and 3,4-dichlorobenzaldehyde in analogy to Example 18. 1H NMR (400 MHz, CDCl3): 8.82-8.81 (m, 2H), 7.98-7.96 (m, 2H), 7.65-7.57 (m, 3H), 7.16-7.13 (m, 1H), 3.88-3.81 (m, 4H), 3.50 (s, 2H), 2.60-2.53 (m, 4H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08530476B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-76269e7c1c064855ac7452c5899bc095 |
| 出典メモ | uspto-grants-2013_09 |