化工社化工社 化学情報印刷レポート · 研究参考用
Piperonal → 4-(1,3-benzodioxol-5-ylmethyl)-N-phenylpiperazine-1-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Piperonal | HCID 8438 | — |
| 反応物 | N-phenylpiperazine-1-carboxamide | HCID 7015289 | — |
| 生成物 | 4-(1,3-benzodioxol-5-ylmethyl)-N-phenylpiperazine-1-carboxamide | HCID 675027 | — |
反応手順
The title compound was prepared from piperazine-1-carboxylic acid phenylamide and benzo[1,3]dioxole-5-carbaldehyde. 1H NMR (400 MHz, CDCl3): 7.36-7.24 (m, 4H), 7.05-6.99 (m, 1H), 6.86 (br s, 1H), 6.77-6.72 (m, 2H), 6.43 (br s, 1H), 5.95 (s, 2H), 3.50-3.46 (m, 4H), 3.43 (s, 2H), 2.46-2.42 (m, 4H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08530476B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-d42b645102fb462481a11dbad67c07ec |
| 出典メモ | uspto-grants-2013_09 |