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3,4-Dimethylbenzaldehyde → 4-(3,4-Dimethyl-benzyl)-piperazine-1-carboxylic acid phenylamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,4-Dimethylbenzaldehyde | HCID 22278 | — |
| 反応物 | N-phenylpiperazine-1-carboxamide | HCID 7015289 | — |
| 生成物 | 4-(3,4-Dimethyl-benzyl)-piperazine-1-carboxylic acid phenylamide | HCID 23822027 | — |
反応手順
The title compound was prepared from piperazine-1-carboxylic acid phenylamide and 3,4-dimethylbenzaldehyde. 1H NMR (400 MHz, CDCl3): 7.35-7.26 (m, 4H), 7.11-7.00 (m, 4H), 6.31 (s, 1H), 3.51-3.48 (m, 6H), 2.49-2.26 (m, 4H), 2.26 (d, J=3.8 Hz, 6H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08530476B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-9643308619de4ba7ae14c3db84a9873a |
| 出典メモ | uspto-grants-2013_09 |