化工社化工社 化学情報印刷レポート · 研究参考用
Triphosgene → 5-Bromo-2-isocyanatomethyl-1,3-dimethyl-benzene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triphosgene | HCID 94429 | — |
| 反応物 | (4-Bromo-2,6-dimethylphenyl)methanamine | HCID 39872008 | — |
| 反応物 | 6-cyclopropyl-6-(2-hydroxy-2-methylpropyl)-3-((S)-1-(4-(1-methyl-2-oxo-1,2-dihydropyridin-4-yl)phenyl)ethyl)-1,3-oxazinan-2-one | HCID 59635673 | — |
| 生成物 | 5-Bromo-2-isocyanatomethyl-1,3-dimethyl-benzene | HCID 58102394 | — |
反応手順
The title compound was prepared from 4-bromo-2,6-dimethyl-benzylamine and triphosgene following a procedure analogous to that described in Step 4 of Intermediate 1. Mass spectrum (EI): m/z=239/241 (Br) [M]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08754076B2 |
| 出典データセット | uspto-grants-2014_06 |
| ORD ID | ord-96f615c1fefb4223bae3942daee0a930 |
| 出典メモ | uspto-grants-2014_06 |