Diethylamine → 2-Diethylamino-4-methylamino-5-nitro-benzoic acid methyl ester
反応式
[CH3:1][O:2][C:3](=[O:16])[C:4]1[CH:9]=[C:8]([N+:10]([O-:12])=[O:11])[C:7]([NH:13][CH3:14])=[CH:6][C:5]=1F.[CH2:17]([NH:19][CH2:20][CH3:21])[CH3:18]>CN(C=O)C>[CH3:1][O:2][C:3](=[O:16])[C:4]1[CH:9]=[C:8]([N+:10]([O-:12])=[O:11])[C:7]([NH:13][CH3:14])=[CH:6][C:5]=1[N:19]([CH2:20][CH3:21])[CH2:17][CH3:18]参加物
4
実験手順
2-Diethylamino-4-methylamino-5-nitro-benzoic acid methyl ester (1.2 g) was prepared by following General Procedure A starting from 2-fluoro-4-methylamino-5-nitro-benzoic acid methyl ester (1.0 g) and diethylamine (683 uL) in DMF.
出典と根拠
- ORDレコード
- ord-4ffcdd68e00b4846a811cb034a0d477b
- 出典データセット
- uspto-grants-2014_06
- 特許番号
- US08759535B2
反応ノート
読み込み中…