化工社化工社 化学情報印刷レポート · 研究参考用
Methylamine → Methyl 4-(methylamino)-3-nitrobenzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methylamine | HCID 6329 | — |
| 反応物 | Methyl 4-chloro-3-nitrobenzoate | HCID 735797 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | Methyl 4-(methylamino)-3-nitrobenzoate | HCID 7650848 | — |
反応手順
4-Methylamino-3-nitro-benzoic acid methyl ester (822 mg) was prepared by following General Procedure A starting from methyl 4-chloro-3-nitrobenzoate (1.0 g) and methylamine (2 M in THF, 6.95 mL) in DMF. The crude product was used in the next step without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08759535B2 |
| 出典データセット | uspto-grants-2014_06 |
| ORD ID | ord-4c0699298eac44c896b94e49de542ae4 |
| 出典メモ | uspto-grants-2014_06 |