化工社化工社 化学情報印刷レポート · 研究参考用
Methyl 4-(methylamino)-3-nitrobenzoate → Methyl 3-amino-4-(methylamino)benzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl 4-(methylamino)-3-nitrobenzoate | HCID 7650848 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 生成物 | Methyl 3-amino-4-(methylamino)benzoate | HCID 15586064 | 96.1% |
反応手順
3-amino-4-methylamino-benzoic acid methyl ester (677 mg) was prepared by following General Procedure B starting from 4-methylamino-3-nitro-benzoic acid methyl ester (822 mg) and Pd/C (10% by weight, 82 mg). The crude product was used in the next step without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08759535B2 |
| 出典データセット | uspto-grants-2014_06 |
| ORD ID | ord-4518beb51d0246db85a61f63cb1016c4 |
| 出典メモ | uspto-grants-2014_06 |