Methylamine → HCID 44518858、化合物

HRID 410955

反応式

HRID 410955 の反応式
F[C:2]1[CH:7]=[CH:6][C:5]([S:8]([CH3:11])(=[O:10])=[O:9])=[CH:4][C:3]=1[N+:12]([O-:14])=[O:13].[CH3:15][NH2:16]>CN(C=O)C>[CH3:11][S:8]([C:5]1[CH:6]=[CH:7][C:2]([CH2:15][NH2:16])=[C:3]([N+:12]([O-:14])=[O:13])[CH:4]=1)(=[O:10])=[O:9]

参加物

4

反応物 2

HCID 6329MethylamineHCID 3131371-Fluoro-4-methanesulfonyl-2-nitrobenzene

生成物 1

HCID 44518858HCID 44518858、化合物

試薬・触媒・溶媒 1

HCID 6228Dimethylformamide溶媒

実験手順

(4-Methanesulfonyl-2-nitro-phenyl)methyl-amine (182 mg) was prepared by following General Procedure A starting from 1-fluoro-4-methanesulfonyl-2-nitro-benzene (219 mg) and methylamine (2 M in THF, 1.0 ml) in DMF (5 mL). The crude product was used in the next step without further purification.

後処理

  1. customThe crude product was used in the next step without further purification

出典と根拠

ORDレコード
ord-a2c85c829b5f41c3b433ff9774433725
出典データセット
uspto-grants-2014_06
特許番号
US08759535B2

関連ノート

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