Methylamine → HCID 67333354、化合物

反応式

Cl[C:2]1[CH:3]=[C:4]([CH2:11][C:12]([NH2:14])=[O:13])[CH:5]=[CH:6][C:7]=1[N+:8]([O-:10])=[O:9].[CH3:15][NH2:16]>>[CH3:15][NH:16][C:2]1[CH:3]=[C:4]([CH2:11][C:12]([NH2:14])=[O:13])[CH:5]=[CH:6][C:7]=1[N+:8]([O-:10])=[O:9]

参加物

反応物 2

HCID 6329Methylamine

HCID 15019103-Chloro-4-nitrophenylacetamide

生成物 1

HCID 67333354HCID 67333354、化合物

実験手順

2-(3-Methylamino-4-nitro-phenyl)-acetamide (727.0 mg) was prepared by following General Procedure A beginning with 2-(3-chloro-4-nitro-phenyl)-acetamide (1.0 g) in methylamine (2.0 M in THF, 20 mL). The crude product was used in the next step without further purification.

後処理

customThe crude product was used in the next step without further purification

出典と根拠

ORDレコード: ord-8987ba9200b84c929c22af461ea5a2a3
出典データセット: uspto-grants-2014_06
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08759535B2

反応ノート

読み込み中…

参加物