化工社化工社 化学情報印刷レポート · 研究参考用
N-Dimethylcarbamoylmethyl-4-methylamino-3-nitro-benzamide → 3-Amino-N-dimethylcarbamoylmethyl-4-methylamino-benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-Dimethylcarbamoylmethyl-4-methylamino-3-nitro-benzamide | HCID 9303598 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 3-Amino-N-dimethylcarbamoylmethyl-4-methylamino-benzamide | HCID 67333499 | 98% |
反応手順
3-Amino-N-dimethylcarbamoylmethyl-4-methylamino-benzamide (700 mg) was prepared by following General Procedure B starting from N-dimethylcarbamoylmethyl-4-methylamino-3-nitro-benzamide (800 mg) and Pd—C (160 mg) in methanol (10 mL).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08759535B2 |
| 出典データセット | uspto-grants-2014_06 |
| ORD ID | ord-d890142553bc4e598c7639be7b6c4c30 |
| 出典メモ | uspto-grants-2014_06 |