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Cyclopropaneacetic acid → N-(Cyclopropylacetyl)-L-alanine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclopropaneacetic acid | HCID 138440 | — |
| 反応物 | Alanine methyl ester hydrochloride | HCID 2733257 | — |
| 生成物 | N-(Cyclopropylacetyl)-L-alanine | HCID 54556694 | — |
反応手順
Following General Procedure A above using cyclopropylacetic acid (Aldrich) and L-alanine methyl ester hydrochloride (Sigma), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.15 in 25% ethyl acetate/hexanes) and purification was by flash column chromatography using 25% ethyl acetate/hexanes as the eluant.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06559141B2 |
| 出典データセット | uspto-grants-2003_05 |
| ORD ID | ord-24afcc70692944019e77012c75949711 |
| 出典メモ | uspto-grants-2003_05 |