化工社化工社 化学情報印刷レポート · 研究参考用
Isobutyl pyruvate → N-(4-azidophenyl)alanine Iso-butyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isobutyl pyruvate | HCID 83084 | — |
| 反応物 | 4-Azidoaniline | HCID 84674 | — |
| 生成物 | N-(4-azidophenyl)alanine Iso-butyl Ester | HCID 54176542 | — |
反応手順
Following General Procedure AA above and using 4-azidoaniline (Aldrich) and iso-butyl pyruvate (prepared by following General Procedure AO above), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.3 in 25% EtOAc/hexanes) and purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06559141B2 |
| 出典データセット | uspto-grants-2003_05 |
| ORD ID | ord-882b12eb691540ff82b4e9ad38f8502c |
| 出典メモ | uspto-grants-2003_05 |