化工社化工社 化学情報印刷レポート · 研究参考用
Phenylacetic Acid → 2-(phenylacetamido)butyric Acid Iso-butyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenylacetic Acid | HCID 999 | — |
| 反応物 | Isobutyl 2-aminobutyrate | HCID 13743360 | — |
| 生成物 | 2-(phenylacetamido)butyric Acid Iso-butyl Ester | HCID 54176777 | — |
反応手順
Following General Procedure BH above and using phenylacetic acid (Aldrich) and iso-butyl 2-aminobutyrate (prepared following General Procedure BJ above), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by chromatography on silica gel using 9:1 toluene:EtOAc as the eluant.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06559141B2 |
| 出典データセット | uspto-grants-2003_05 |
| ORD ID | ord-d5307a4b2fa14eb1a255c949d2021ca3 |
| 出典メモ | uspto-grants-2003_05 |