化工社化工社 化学情報印刷レポート · 研究参考用
L-Alanine ethyl ester → N-[(2-phenyl)-2-fluoroacetyl]alanine Ethyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | L-Alanine ethyl ester | HCID 76507 | — |
| 反応物 | Fluorophenylacetic acid | HCID 102649 | — |
| 生成物 | N-[(2-phenyl)-2-fluoroacetyl]alanine Ethyl Ester | HCID 22894970 | — |
反応手順
Following General Procedure BF above, and using α-fluorophenyl acetic acid (Aldrich) and alanine ethyl ester (Aldrich), the title compound was prepared. The reaction was monitored by tlc on silica gel (Rf=0.75 in 1:1 EtOAc:hexane) and purification was by chromatography on silica gel using 1:2 ethyl acetate/hexanes as the eluent.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06559141B2 |
| 出典データセット | uspto-grants-2003_05 |
| ORD ID | ord-260dd8e9da00468792f4f9025a0a99e9 |
| 出典メモ | uspto-grants-2003_05 |