Sulfuric Acid → 6-Chlorohexanoic acid

反応式

[C:1]([OH:8])(=[O:7])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].S(=O)(=O)(O)O.[Cl:14]Cl>>[Cl:14][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][C:1]([OH:8])=[O:7]

参加物

反応物 3

HCID 1118Sulfuric Acid

HCID 8892Hexanoic Acid

HCID 24526Chlorine

生成物 1

HCID 202096-Chlorohexanoic acid

実験手順

144 parts by mass of the caproic acid were added to 1,000 parts by mass of 27N sulfuric acid saturated with chlorine and were reacted for 6 hours at 25° C. to obtain 93 parts by mass of 6-chlorocaproic acid.

後処理

customwere reacted for 6 hours at 25° C.

出典と根拠

ORDレコード: ord-9116af33c41d4c14b9a4214b1addbdbd
出典データセット: uspto-grants-2003_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06559275B2

反応ノート

読み込み中…