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Water → Furan-2-acetic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 2-Furanacetonitrile | HCID 10909515 | — |
| 生成物 | Furan-2-acetic acid | HCID 75974 | — |
反応手順
A mixture of 2-furanacetonitrile (6.14 g), KOH (4.0 g), and water (25 mL) was refluxed for 1 hour and then cooled. Following extraction with ether, the aqueous layer was acidified to pH 2.0 with concentrated aqueous HCl. This solution was extracted with ether, and the organic phase was dried over MgSO4 and evaporated under vacuum to yield 2-furanacetic acid. The structure of the product was confirmed by NMR.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06566508B2 |
| 出典データセット | uspto-grants-2003_05 |
| ORD ID | ord-dc1b7ed696e7453f8c2cfc7d65c6a3d5 |
| 出典メモ | uspto-grants-2003_05 |